Instrument Catalog
500 MHz wide-bore NMR spectrometer.
3.2 mm CPMAS probe normally installed for solid-state NMR experiments.
Micro MRI imaging capabilities
2 channel system with AS7620 96-sample changer. OneNMR
probe with auto-tune-and-match installed.
Undergraduates have priority on this instrument during lab periods.
Guides and Standard Operating Procedures
Best experiments:
- PROTON
- COSY
- Other nuclei: F19 (no H1 decoupling), P31, B11, (others by request)
Acceptable experiments:
- C13CPD (night time)
- 2D HSQC and HMBC experiments
- 1D/2D NOE experiments
Not available:
- Variable Temperature experiments
- Kinetics experiments
- Simultaneous F19 and H1 experiments
Time Required for NMR Experiments on A400a:
Mass | Concentration | Proton | Carbon | gCOSY | gHSQC | gHMBC |
0.03 mg | 0.1 mM | 10 h 40 min | 35389 hours | 1785 hours | 1886 hours | 7129 hours |
0.06 mg | 0.2 mM | 2 h 40 min | 10516 hours | 46 h 28 min | 474 h 12 min | 1785 hours |
0.15 mg | 0.5 mM | 0 h 26 min | 1415 h 33 min | 6 h 10 min | 75 h 01 min | 284 h 44 min |
0.3 mg | 1 mM | 0 h 06 min | 354 h 01 min | 1 h 40 min | 18 h 53 min | 71 h 19 min |
0.6 mg | 2 mM | 0 h 01 min | 88 h 31 min | 0 h 26 min | 4 h 42 min | 17 h 51 min |
1.5 mg | 5 mM | < 1 min | 14 h 09 min | 0 h 03 min | 0 h 45 min | 2 h 51 min |
3 mg | 10 mM | < 1 min | 3 h 32 min | 0 h 03 min | 0 h 16 min | 1 h 07 min |
6 mg | 20 mM | < 1 min | 0 h 53 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
12 mg | 40 mM | < 1 min | 0 h 13 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
15 mg | 50 mM | < 1 min | 0 h 08 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
> 30 mg | 100+ mM | < 1 min | 0 h 04 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
All estimates based on a 500 MW sample in 600 uL solvent volume using a 5 mm diameter NMR tube
2 channel system. AutoX DB probe installed. Variable-temperature and H/F experiments available.
Guides and Standard Operating Procedures
Best experiments:
- PROTON
- Simultaneous F19 and H1 experiments (i.e. F19 with H1 decoupling)
- Variable Temperature experiments (with appropriate CBIC training)
- Kinetics experiments
Acceptable experiments:
- C13CPD
- 2D HSQC and HMBC experiments
- 1D/2D NOE experiments
Not available:
- Nuclei other than H1, F19 & C13
Time Required for NMR Experiments on A400b:
Mass | Concentration | Proton | Carbon | gCOSY | gHSQC | gHMBC |
0.03 mg | 0.1 mM | 44 h 44 min | 50960 hours | 644 hours | 7862 hours | 29844 hours |
0.06 mg | 0.2 mM | 11 h 11 min | 12740 hours | 161 hours | 1965 hours | 7461 hours |
0.15 mg | 0.5 mM | 1 h 47 min | 2038 h 24 min | 25 h 47 min | 319 h 18 min | 1193 h 57 min |
0.3 mg | 1 mM | 0 h 27 min | 509 h 36 min | 6 h 30 min | 78 h 37 min | 298 h 40 min |
0.6 mg | 2 mM | 0 h 07 min | 127 h 27 min | 1 h 38 min | 19 h 48 min | 75 h 40 min |
1.5 mg | 5 mM | 0 h 01 min | 20 h 23 min | 0 h 16 min | 3 h 08 min | 12 h 15 min |
3 mg | 10 mM | < 1 min | 5 h 15 min | 0 h 06 min | 0 h 47 min | 1 h 32 min |
6 mg | 20 mM | < 1 min | 1 h 16 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
12 mg | 40 mM | < 1 min | 0 h 19 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
15 mg | 50 mM | < 1 min | 0 h 12 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
> 30 mg | 100+ mM | < 1 min | 0 h 04 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
All estimates based on a 500 MW sample in 600 uL solvent volume using a 5 mm diameter NMR tube
2 channel system with AS7620 96-sample changer. OneNMR probe with auto-tune-and-match installed.
Primarily used for short, routine NMR experiments where data is needed quickly.
Guides and Standard Operating Procedures
Best experiments:
- PROTON
- COSY
- Other nuclei: F19 (no H1 decoupling), P31, B11, (others by request)
Acceptable experiments:
- C13CPD (night time)
- 2D HSQC and HMBC experiments (night time)
- 1D/2D NOE experiments (night time)
Not available:
- Variable Temperature experiments
- Kinetics experiments
- Simultaneous F19 and H1 experiments
Time Required for NMR Experiments on A400c:
Mass | Concentration | Proton | Carbon | gCOSY | gHSQC | gHMBC |
0.03 mg | 0.1 mM | 10 h 40 min | 35389 hours | 1785 hours | 1886 hours | 7129 hours |
0.06 mg | 0.2 mM | 2 h 40 min | 10516 hours | 46 h 28 min | 474 h 12 min | 1785 hours |
0.15 mg | 0.5 mM | 0 h 26 min | 1415 h 33 min | 6 h 10 min | 75 h 01 min | 284 h 44 min |
0.3 mg | 1 mM | 0 h 06 min | 354 h 01 min | 1 h 40 min | 18 h 53 min | 71 h 19 min |
0.6 mg | 2 mM | 0 h 01 min | 88 h 31 min | 0 h 26 min | 4 h 42 min | 17 h 51 min |
1.5 mg | 5 mM | < 1 min | 14 h 09 min | 0 h 03 min | 0 h 45 min | 2 h 51 min |
3 mg | 10 mM | < 1 min | 3 h 32 min | 0 h 03 min | 0 h 16 min | 1 h 07 min |
6 mg | 20 mM | < 1 min | 0 h 53 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
12 mg | 40 mM | < 1 min | 0 h 13 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
15 mg | 50 mM | < 1 min | 0 h 08 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
> 30 mg | 100+ mM | < 1 min | 0 h 04 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
All estimates based on a 500 MW sample in 600 uL solvent volume using a 5 mm diameter NMR tube
2 channel system, OneNMR probe with auto-tune-and-match installed.
Guides and Standard Operating Procedures
Best experiments:
- PROTON
- COSY
- 2D HSQC and HMBC experiments
- 1D/2D NOE experiments
- Other nuclei: F19 (no H1 decoupling), P31, B11, (others by request)
- Variable Temperature experiments
- Kinetics experiments
Acceptable experiments:
- C13CPD
Not available:
- Simultaneous F19 and H1 experiments
Time Required for NMR Experiments on A500a:
Mass | Concentration | Proton | Carbon | gCOSY | gHSQC | gHMBC |
0.03 mg | 0.1 mM | 5 hours | 16962 hours | 67 h 16 min | 820 h 42 min | 3113 h 37 min |
0.06 mg | 0.2 mM | 1 h 10 min | 424 h 02 min | 16 h 50 min | 205 h 15 min | 779 h 06 min |
0.15 mg | 0.5 mM | 0 h 11 min | 678 h 28 min | 2 h 45 min | 32 h 50 min | 124 h 34 min |
0.3 mg | 1 mM | 0 h 03 min | 170 h 00 min | 0 h 42 min | 8 h 20 min | 31 h 09 min |
0.6 mg | 2 mM | < 1 min | 4 h 15 min | 0 h 11 min | 2 h 05 min | 7 h 48 min |
1.5 mg | 5 mM | < 1 min | 3 h 11 min | 0 h 03 min | 0 h 08 min | 1 h 40 min |
3 mg | 10 mM | < 1 min | 1 h 42 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
6 mg | 20 mM | < 1 min | 0 h 25 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
12 mg | 40 mM | < 1 min | 0 h 06 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
15 mg | 50 mM | < 1 min | 0 h 04 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
> 30 mg | 100+ mM | < 1 min | 0 h 04 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
All estimates based on a 500 MW sample in 600 uL solvent volume using a 5 mm diameter NMR tube
2 channel system, OneNMR probe with auto-tune-and-match installed.
Guides and Standard Operating Procedures
Best experiments:
- PROTON
- COSY
- 2D HSQC and HMBC experiments
- 1D/2D NOE experiments
- Other nuclei: F19 (no H1 decoupling), P31, B11, (others by request)
- Variable Temperature experiments
- Kinetics experiments
Acceptable experiments:
- C13CPD
Not available:
- Simultaneous F19 and H1 experiments
Time Required for NMR Experiments on A500b:
Mass | Concentration | Proton | Carbon | gCOSY | gHSQC | gHMBC |
0.03 mg | 0.1 mM | 5 hours | 16962 hours | 67 h 16 min | 820 h 42 min | 3113 h 37 min |
0.06 mg | 0.2 mM | 1 h 10 min | 424 h 02 min | 16 h 50 min | 205 h 15 min | 779 h 06 min |
0.15 mg | 0.5 mM | 0 h 11 min | 678 h 28 min | 2 h 45 min | 32 h 50 min | 124 h 34 min |
0.3 mg | 1 mM | 0 h 03 min | 170 h 00 min | 0 h 42 min | 8 h 20 min | 31 h 09 min |
0.6 mg | 2 mM | < 1 min | 4 h 15 min | 0 h 11 min | 2 h 05 min | 7 h 48 min |
1.5 mg | 5 mM | < 1 min | 3 h 11 min | 0 h 03 min | 0 h 08 min | 1 h 40 min |
3 mg | 10 mM | < 1 min | 1 h 42 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
6 mg | 20 mM | < 1 min | 0 h 25 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
12 mg | 40 mM | < 1 min | 0 h 06 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
15 mg | 50 mM | < 1 min | 0 h 04 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
> 30 mg | 100+ mM | < 1 min | 0 h 04 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
All estimates based on a 500 MW sample in 600 uL solvent volume using a 5 mm diameter NMR tube
3 channel system with AS7510 12-sample automatic sample changer. C{H} cold probe with auto-tune-and-match installed. Highest sensitivity for C13 NMR experiments.
Guides and Standard Operating Procedures
Best experiments:
- CARBON
- PROTON
Acceptable experiments:
- 1D/2D NOE experiments
Not available:
- Variable Temperature experiments
- Kinetics experiments
- Nuclei other than H1 and C13
Time Required for NMR Experiments on A600a:
Mass | Concentration | Proton | Carbon | gCOSY | gHSQC | gHMBC |
0.03 mg | 0.1 mM | 0 h 24 min | 1298 hours | 5 h 54 min | 72 h 04 min | 272 h 22 min |
0.06 mg | 0.2 mM | 0 h 06 min | 324 h 32 min | 1 h 28 min | 19 h 35 min | 68 h 32 min |
0.15 mg | 0.5 mM | 0 h 01 min | 51 h 56 min | 0 h 16 min | 3 h 11 min | 11 h 10 min |
0.3 mg | 1 mM | < 1 min | 13 h 00 min | 0 h 03 min | 0 h 47 min | 2 h 47 min |
0.6 mg | 2 mM | < 1 min | 3 h 15 min | 0 h 03 min | 0 h 16 min | 1 h 07 min |
1.5 mg | 5 mM | < 1 min | 0 h 31 min | 0 h 03 min | 0 h 08 min | 0 h 34 min |
3 mg | 10 mM | < 1 min | 0 h 08 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
6 mg | 20 mM | < 1 min | 0 h 04 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
12 mg | 40 mM | < 1 min | 0 h 04 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
15 mg | 50 mM | < 1 min | 0 h 04 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
> 30 mg | 100+ mM | < 1 min | 0 h 04 min | 0 h 03 min | 0 h 08 min | 0 h 17 min |
All estimates based on a 500 MW sample in 600 uL solvent volume using a 5 mm diameter NMR tube
4 channel system. Inverse-detect HCN probe, Dual Band (direct-detect) probe, and H{CN} C13-sensitivity enhanced salt-tolerant cold probe available.
Experienced Users Only. Contact CBIC staff for more information.
X-Band Electron Paramagnetic Resonance. Equipped with a cryogen-free cryostat.
3 channel system. Inverse-detect HCN probe installed.
3 channel system. Inverse-detect HCN probe installed.