A600a Agilent DD2 600 MHz NMR Spectrometer (Autosampler)

Short Name: 
A600a
Instrument Type: 
NMR & EPR
Location: 
KCL 3
Date of Acquisition: 
October 2013
Description: 

3 channel system with AS7510 12-sample automatic sample changer. C{H} cold probe with auto-tune-and-match installed. Highest sensitivity for C13 NMR experiments.

Best experiments:

  • CARBON
  • PROTON

Acceptable experiments:

  • 1D/2D NOE experiments

Not available:

  • Variable Temperature experiments
  • Kinetics experiments
  • Nuclei other than H1 and C13

Time Required for NMR Experiments on A600a:

Mass Concentration Proton Carbon gCOSY  gHSQC gHMBC
0.03 mg 0.1 mM 0 h 24 min 1298 hours 5 h 54 min 72 h 04 min 272 h 22 min
0.06 mg 0.2 mM 0 h 06 min 324 h 32 min 1 h 28 min 19 h 35 min 68 h 32 min
0.15 mg 0.5 mM 0 h 01 min 51 h 56 min 0 h 16 min 3 h 11 min 11 h 10 min
0.3 mg 1 mM < 1 min 13 h 00 min 0 h 03 min 0 h 47 min 2 h 47 min
0.6 mg 2 mM < 1 min 3 h 15 min 0 h 03 min 0 h 16 min 1 h 07 min
1.5 mg 5 mM < 1 min 0 h 31 min 0 h 03 min 0 h 08 min 0 h 34 min
3 mg 10 mM < 1 min 0 h 08 min 0 h 03 min 0 h 08 min 0 h 17 min
6 mg 20 mM < 1 min 0 h 04 min 0 h 03 min 0 h 08 min 0 h 17 min
12 mg 40 mM < 1 min 0 h 04 min 0 h 03 min 0 h 08 min 0 h 17 min
15 mg 50 mM < 1 min 0 h 04 min 0 h 03 min 0 h 08 min 0 h 17 min
> 30 mg 100+ mM < 1 min 0 h 04 min 0 h 03 min 0 h 08 min 0 h 17 min

All estimates based on a 500 MW sample in 600 uL solvent volume using a 5 mm diameter NMR tube

Instrument Image: